394904
ペンタフルオロプロピオン酸無水物
derivatization grade (GC derivatization), LiChropur™, 99%
別名:
PFPA, パーフルオロプロピオン酸無水物
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この商品について
化学式:
(CF3CF2CO)2O
CAS番号:
分子量:
310.05
UNSPSC Code:
23151817
NACRES:
NA.22
PubChem Substance ID:
EC Number:
206-604-2
Beilstein/REAXYS Number:
1806446
MDL number:
Assay:
99%
Form:
liquid
grade
derivatization grade (GC derivatization)
Quality Level
assay
99%
form
liquid
quality
LiChropur™
reaction suitability
reagent type: derivatization reagent
reaction type: Acylations
technique(s)
gas chromatography (GC): suitable
bp
69-70 °C/735 mmHg (lit.)
density
1.571 g/mL at 25 °C (lit.)
SMILES string
FC(F)(F)C(F)(F)C(=O)OC(=O)C(F)(F)C(F)(F)F
InChI
1S/C6F10O3/c7-3(8,5(11,12)13)1(17)19-2(18)4(9,10)6(14,15)16
InChI key
XETRHNFRKCNWAJ-UHFFFAOYSA-N
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関連するカテゴリー
Application
Learn more in the Product Information
Derivatization reagent used in a GC-MS analysis of stereoisomer content of synthetic peptides. Also used in a GC-MS detection method for synephrine in dietary supplements.
For the preparation of volatile pentafluoropropionyl derivatives of a wide range of compounds, for example, amines and alcohols, for EC/GC.
Pentafluoropropionic anhydride (PFPA) was used as derivatization reagent for urine samples to determine the presence of codeine, morphine, 6-monoacetylmorphine, ethylmorphine, and dihydrocodeine using GC-MS in selected ion monitoring (SIM) mode. It was also used to derivatize the dry pericardial fluid sample extracts for quantification of cocaine, benzoylecgonine, and cocaethylene in pericardial fluid using GC-MS.
Packaging
Clear borosilicate glass, high hydrolytic resistance (Type I)
Legal Information
LiChropur is a trademark of Merck KGaA, Darmstadt, Germany
signalword
Danger
hcodes
Hazard Classifications
Skin Corr. 1B
supp_hazards
保管分類
8A - Combustible corrosive hazardous materials
wgk
WGK 3
flash_point_f
Not applicable
flash_point_c
Not applicable
ppe
Faceshields, Gloves, Goggles, type ABEK (EN14387) respirator filter
適用法令
試験研究用途を考慮した関連法令を主に挙げております。化学物質以外については、一部の情報のみ提供しています。 製品を安全かつ合法的に使用することは、使用者の義務です。最新情報により修正される場合があります。WEBの反映には時間を要することがあるため、適宜SDSをご参照ください。
394904-10ML: + 394904-10X1ML: + 394904-25ML: + 394904-INTR: + 394904-100ML: + 394904-VAR: + 394904-1ML: + 394904-5ML: + 394904-BULK:
jan
Emilia Marchei et al.
Journal of pharmaceutical and biomedical analysis, 41(4), 1468-1472 (2006-05-16)
A simple and rapid procedure based on gas chromatography-mass spectrometry (GC-MS) is described for determination of synephrine, active principle of Citrus aurantium plant, in solid and liquid dietary supplements. After the addition of 3,4-methylenedioxypropylamphetamine as internal standard (I.S.), a liquid-liquid
Ralf Pätzold et al.
Chirality, 18(7), 551-557 (2006-05-10)
Synthetic dipeptides comprising mixtures of enantiomers, diastereomers, or sequential isomers were converted into their N-perfluoroacetyl dipeptide esters (perfluoroacetyl: trifluoroacetyl, pentafluoroacetyl, heptafluorobutyryl; ester: methyl, 1-propyl, 2-propyl, 2,2,2-trifluoroethyl) and analyzed by GC-MS on the chiral stationary phases Chirasil-L-Val and Lipodex-E using helium
Comparison of RapiTest? with Emit? d, au? and GC-MS for the Analysis of Drugs in Urine.
Korte, T., et al.
Journal of Analytical Toxicology, 21, 49-53 (1997)
María Teresa Contreras et al.
Journal of analytical toxicology, 31(2), 75-80 (2007-06-01)
A method is described for the simultaneous quantification of cocaine, benzoylecgonine, and cocaethylene in pericardial fluid. Pericardial fluid samples from autopsy casework involving cocaine-related deaths and deaths unrelated to drug abuse were collected. The extraction of cocaine and its metabolites
Ju-Yeon Moon et al.
Journal of lipid research, 52(8), 1595-1603 (2011-05-24)
Estrogen metabolites play important roles in the development of female-related disorders and homeostasis of the bone. To improve detectability, a validated gas chromatography-mass spectrometry (GC-MS) method was conducted with two-phase extractive ethoxycarbonlyation (EOC) and subsequent pentafluoropropionyl (PFP) derivatization was introduced.
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